{"code":"SASDAA8","status":"Published","type_of_curve":"Single concentration","angular_unit":"1/nm","project":{"title":"Accuracy of molecular mass determination of proteins in solution by small-angle X-ray scattering","publication":{"title":"Accuracy of molecular mass determination of proteins in solution by small-angle X-ray scattering","author_list":"Mylonas E, Svergun D","journal":"Journal of Applied Crystallography","doi":"10.1107/S002188980700252X","pmid":null,"published_date":"2007 Feb 17"},"status":"released","submitted_date":"2015-07-06","released_date":"2015-07-07"},"pddf_data":"https://www.sasbdb.org/media/p_of_R_files/SASDAA8.out","intensities_data":"https://www.sasbdb.org/media/intensities_files/SASDAA8.dat","intensities_log_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDAA8_dat_img.png","intensities_kratky_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDAA8_kratky_img.png","pddf_plot":"https://www.sasbdb.org/media/p_of_R_files/pofr_images/SASDAA8_pofr_img.png","intensities_guinier_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDAA8_guinier_img.png","sascif_data":"https://www.sasbdb.org/media/sascif/sascif_files/SASDAA8.sascif","experiment":{"instrument":{"detector":{"type":null,"name":"MAR 345 Image Plate","resolution":null},"name":"DORIS III, DESY","city":"Hamburg","country":"Germany","beamline_name":"EMBL X33","beam_geometry":null,"type_of_source":"X-ray synchrotron","point_source":null,"line_collimation":null,"sample_path_length":null,"line_collimation_slitlength":null,"line_collimation_integrationwidth":null,"xray_energy":null,"beam_profile_ah":null,"beam_profile_al":null},"sample":{"molecule":[{"long_name":"Chymotrypsinogen A","short_name":null,"sequence":"CGVPAIQPVLSGLSRIVNGEEAVPGSWPWQVSLQDKTGFHFCGGSLINENWVVTAAHCGVTTSDVVVAGEFDQGSSSEKIQKLKIAKVFKNSKYNSLTINNDITLLKLSTAASFSQTVSAVCLPSASDDFAAGTTCVTTGWGLTRYTNANTPDRLQQASLPLLSNTNCKKYWGTKIKDAMICAGASGVSSCMGDSGGPLVCKKNGAWTLVGIVSWGSSTCSTSTPGVYARVTALVNWVQQTLAAN","organism":"Bos taurus","uniprot_code":"P00766","uniprot_range_first":null,"uniprot_range_last":null,"oligomerization":"monomer","molecular_type":"protein","uniprot_sequence":"CGVPAIQPVLSGLSRIVNGEEAVPGSWPWQVSLQDKTGFHFCGGSLINENWVVTAAHCGV\nTTSDVVVAGEFDQGSSSEKIQKLKIAKVFKNSKYNSLTINNDITLLKLSTAASFSQTVSA\nVCLPSASDDFAAGTTCVTTGWGLTRYTNANTPDRLQQASLPLLSNTNCKKYWGTKIKDAM\nICAGASGVSSCMGDSGGPLVCKKNGAWTLVGIVSWGSSTCSTSTPGVYARVTALVNWVQQ\nTLAAN","mw":25.666,"total_mw":25.666,"number_molecules":1,"complex_state":false,"deuteration":null,"molecule_source":"biological","molecule_description":null}],"buffer":{"name":"100 mM Tris/HCl 100 mM NaCl","concentration_unit":"mM","comment":null,"additive":"100 mM NaCl","concentration":100.0,"pka":null,"ph":7.5,"deuteration":null},"purity_method":null,"name":"Chymotrypsinogen A in Tris/HCl ","ext_coefficient":null,"contrast":null,"specific_vol":null,"dry_vol":null,"absorbption":null,"deuteration":null,"mixture":null},"contributor":[{"affiliation":[{"short_name":"EMBL-Hamburg","address":"Notkestraße 85, Geb. 25A, 22607 Hamburg, Deutschland, Germany","full_name":"European Molecular Biology Laboratory (EMBL) - Hamburg outstation","webpage":"http://www.embl-hamburg.de/index.php"},{"short_name":"FORTH","address":"Heraklion, Greece","full_name":"Foundation for Research and Technology-Hellas","webpage":"http://www.forth.gr/index.php?l=e"}],"contributor_name":"Efstratios","contributor_surname":"Mylonas","orcid":null}],"concentration_method":null,"concentration_unit":"mg/ml","date":"2006-05-19","storage_temperature":null,"cell_temperature":20.0,"exposure_time":null,"number_of_frames":null,"wavelength":null,"sample_detector_distance":null,"concentration_min":null,"concentration_max":6.02,"sample_volume":null,"flow_rate":null,"s_min":0.081,"s_max":4.956,"total_exposure_time":null,"seccolumn":null},"fits":[{"models":[{"model_plot":"https://www.sasbdb.org/media/pdb_file/images/SASDAA8_fit1_model1_img.png","software":"CRYSOL","pdb_link":[],"model_title":null,"type_of_model":"atomic","software_version":"","model_data":"https://www.sasbdb.org/media/pdb_file/SASDAA8_fit1_model1.pdb","model_mw":25.67,"bead_radius":1.9,"log":null,"symmetry":"","comment":"","user":61}],"fit_unit":"1/A","fit_plot":"https://www.sasbdb.org/media/fitting_files/scattering_plots/SASDAA8_fit1_fixed_fit_img.png","software":"CRYSOL","chi_square_value":4.247721,"p_value":0.0,"fit_residual_plot":"SASDAA8_fit1_fitresiduals_img.png","fit_data":"https://www.sasbdb.org/media/fitting_files/SASDAA8_fit1.fit","fit_log":null,"software_version":"","description":null}],"estimated_volume_method":null,"pddf_software":"ATSAS GNOM","pddf_software_version":null,"i0_calibration_standard":null,"description":null,"experiment_description":null,"tags":["benchmark","X33"],"intensity_unit":null,"experimental_mw":25.7,"experimental_mw_error":null,"guinier_i0_mw":25.7,"guinier_i0_mw_error":null,"porod_mw":null,"porod_mw_error":null,"pddf_i0":83.0,"pddf_i0_error":null,"guinier_i0":87.52,"guinier_i0_error":null,"pddf_rg":1.74,"pddf_rg_error":null,"guinier_rg":1.87,"guinier_rg_error":null,"pddf_dmax":5.0,"pddf_dmax_error":null,"porod_volume":null,"porod_volume_error":null,"estimated_volume":null,"estimated_volume_error":null,"guinier_point_first":81,"guinier_point_last":232,"pddf_point_first":null,"pddf_point_last":null,"i0_calibration_standard_data":null,"intensities_log_log_plot":"SASDAA8_datloglog_img.png","symmetry":null,"last_modified":"2023-05-25T11:22:16.556436+02:00","bragg_peak":[]}