{"code":"SASDDF3","status":"Published","type_of_curve":"Single concentration","angular_unit":"1/A","project":{"title":"Structural Study of the Complex Formed by Ceruloplasmin and Macrophage Migration Inhibitory Factor.","publication":{"title":"Structural Study of the Complex Formed by Ceruloplasmin and Macrophage Migration Inhibitory Factor.","author_list":"Sokolov AV, Dadinova LA, Petoukhov MV, Bourenkov G, Dubova KM, Amarantov SV, Volkov VV, Kostevich VA, Gorbunov NP, Grudinina NA, Vasilyev VB, Samygina VR","journal":"Biochemistry (Mosc)","doi":"10.1134/S000629791806007X","pmid":"30195326","published_date":"2018 Jun"},"status":"released","submitted_date":"2018-02-06","released_date":"2018-02-08"},"pddf_data":"https://www.sasbdb.org/media/p_of_R_files/SASDDF3.out","intensities_data":"https://www.sasbdb.org/media/intensities_files/SASDDF3.dat","intensities_log_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDDF3_dat_img.png","intensities_kratky_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDDF3_kratky_img.png","pddf_plot":"https://www.sasbdb.org/media/p_of_R_files/pofr_images/SASDDF3_pofr_img.png","intensities_guinier_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDDF3_guinier_img.png","sascif_data":"https://www.sasbdb.org/media/sascif/sascif_files/SASDDF3.sascif","experiment":{"instrument":{"detector":{"type":"linear","name":"Braun OED 50M position-sensitive","resolution":0.0},"name":null,"city":"Moscow","country":"Russian Federation","beamline_name":"HECUS System-3","beam_geometry":null,"type_of_source":"X-ray in 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CuSO4, 100mM Hepes","concentration_unit":null,"comment":null,"additive":null,"concentration":null,"pka":null,"ph":7.4,"deuteration":null},"purity_method":null,"name":"Macrophage migration inhibitory factor bound to Ceruloplasmin (MIF-CP complex)","ext_coefficient":null,"contrast":null,"specific_vol":null,"dry_vol":null,"absorbption":null,"deuteration":null,"mixture":null},"contributor":[{"affiliation":[{"short_name":"MSU","address":"Moscow, Russia","full_name":"Lomonosov Moscow State University","webpage":"http://www.msu.ru"}],"contributor_name":"Liubov","contributor_surname":"Dadinova","orcid":null}],"concentration_method":null,"concentration_unit":null,"date":"2015-12-22","storage_temperature":20.0,"cell_temperature":20.0,"exposure_time":5400.0,"number_of_frames":1,"wavelength":0.154,"sample_detector_distance":0.28,"concentration_min":5.0,"concentration_max":10.0,"sample_volume":null,"flow_rate":null,"s_min":0.191,"s_max":2.488,"total_exposure_time":null,"seccolumn":null},"fits":[{"models":[{"model_plot":"https://www.sasbdb.org/media/pdb_file/images/SASDDF3_fit1_model1_img.png","software":"ClusPro","pdb_link":[],"model_title":null,"type_of_model":"atomic","software_version":null,"model_data":"https://www.sasbdb.org/media/pdb_file/SASDDF3_fit1_model1.pdb","model_mw":155.1,"bead_radius":1.9,"log":null,"symmetry":null,"comment":null,"user":35}],"fit_unit":"1/A","fit_plot":"https://www.sasbdb.org/media/fitting_files/scattering_plots/SASDDF3_fit1_fit_img.png","software":"CRYSOL","chi_square_value":2.224,"p_value":0.004219,"fit_residual_plot":"SASDDF3_fit1_fitresiduals_img.png","fit_data":"https://www.sasbdb.org/media/fitting_files/SASDDF3_fit1.fit","fit_log":"https://www.sasbdb.org/media/fitting_files/log_files/model202.log","software_version":"5,0","description":null}],"estimated_volume_method":null,"pddf_software":"ATSAS 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Solute concentrations ranging between 5 and 10 mg/ml were measured at 20°C. One 5400 second frame was collected. The data were normalized to the intensity of the transmitted beam and radially averaged; the scattering of the solvent-blank was subtracted.","tags":[],"intensity_unit":"arbitrary","experimental_mw":138.0,"experimental_mw_error":null,"guinier_i0_mw":138.0,"guinier_i0_mw_error":7.0,"porod_mw":142.5,"porod_mw_error":null,"pddf_i0":14030.0,"pddf_i0_error":1554.0,"guinier_i0":13053.0,"guinier_i0_error":755.0,"pddf_rg":3.94,"pddf_rg_error":0.5,"guinier_rg":3.56,"guinier_rg_error":0.3,"pddf_dmax":14.41,"pddf_dmax_error":0.5,"porod_volume":228.0,"porod_volume_error":null,"estimated_volume":null,"estimated_volume_error":null,"guinier_point_first":4,"guinier_point_last":22,"pddf_point_first":null,"pddf_point_last":null,"i0_calibration_standard_data":null,"intensities_log_log_plot":"SASDDF3_datloglog_img.png","symmetry":null,"last_modified":"2019-12-06T13:07:15.624532+01:00","bragg_peak":[]}