{"code":"SASDDK9","status":"Published","type_of_curve":"Single concentration","angular_unit":"1/A","project":{"title":"Human Dystrophin Structural Changes upon Binding to Anionic Membrane Lipids.","publication":{"title":"Human Dystrophin Structural Changes upon Binding to Anionic Membrane Lipids.","author_list":"Dos Santos Morais R, Delalande O, Pérez J, Mias-Lucquin D, Lagarrigue M, Martel A, Molza AE, Chéron A, Raguénès-Nicol C, Chenuel T, Bondon A, Appavou MS, Le Rumeur E, Combet S, Hubert JF","journal":"Biophys J","doi":"10.1016/j.bpj.2018.07.039","pmid":"30197181","published_date":"2018 Oct 2"},"status":"released","submitted_date":"2018-07-03","released_date":"2018-09-04"},"pddf_data":"https://www.sasbdb.org/media/p_of_R_files/SASDDK9.out","intensities_data":"https://www.sasbdb.org/media/intensities_files/SASDDK9.txt","intensities_log_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDDK9_dat_img.png","intensities_kratky_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDDK9_kratky_img.png","pddf_plot":"https://www.sasbdb.org/media/p_of_R_files/pofr_images/SASDDK9_pofr_img.png","intensities_guinier_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDDK9_guinier_img.png","sascif_data":"https://www.sasbdb.org/media/sascif/sascif_files/SASDDK9.sascif","experiment":{"instrument":{"detector":{"type":"128 linear sensitive multidetector","name":"Reuter-Stokes 3He","resolution":0.8},"name":"Institut Laue-Langevin (ILL)","city":"Grenoble","country":"France","beamline_name":"D22","beam_geometry":null,"type_of_source":"neutron source","point_source":null,"line_collimation":null,"sample_path_length":null,"line_collimation_slitlength":null,"line_collimation_integrationwidth":null,"xray_energy":null,"beam_profile_ah":null,"beam_profile_al":null},"sample":{"molecule":[{"long_name":"R1-3 human dystrophin fragment","short_name":"R1-3","sequence":"GSEVNLDRYQTALEEVLSWLLSAEDTLQAQGEISNDVEVVKDQFHTHEGYMMDLTAHQGRVGNILQLGSKLIGTGKLSEDEETEVQEQMNLLNSRWECLRVASMEKQSNLHRVLMDLQNQKLKELNDWLTKTEERTRKMEEEPLGPDLEDLKRQVQQHKVLQEDLEQEQVRVNSLTHMVVVVDESSGDHATAALEEQLKVLGDRWANICRWTEDRWVLLQDILLKWQRLTEEQCLFSAWLSEKEDAVNKIHTTGFKDQNEMLSSLQKLAVLKADLEKKKQSMGKLYSLKQDLLSTLKNKSVTQKTEAWLDNFARCWDNLVQKLEKSTAQISQA","organism":"Homo 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mM Tris-d11, 150 mM NaCl, 0.1 mM EDTA-d16, in 100% D2O, pD 7.5","concentration_unit":null,"comment":"pD = pH + 04","additive":null,"concentration":null,"pka":null,"ph":7.1,"deuteration":null},"purity_method":null,"name":"Conformation of R1-3 human dystrophin fragment in interaction with zwitterionic phospholipid bicelles (SANS)","ext_coefficient":null,"contrast":null,"specific_vol":null,"dry_vol":null,"absorbption":null,"deuteration":null,"mixture":null},"contributor":[{"affiliation":[{"short_name":null,"address":"France","full_name":"LLB, UMR12 CEA/CNRS","webpage":"http://www-llb.cea.fr/"}],"contributor_name":"Sophie","contributor_surname":"Combet","orcid":"https://orcid.org/0000-0002-8672-4514"}],"concentration_method":null,"concentration_unit":null,"date":"2016-11-07","storage_temperature":4.0,"cell_temperature":22.0,"exposure_time":null,"number_of_frames":null,"wavelength":0.6,"sample_detector_distance":1.4,"concentration_min":null,"concentration_max":4.2,"sample_volume":null,"flow_rate":null,"s_min":0.065,"s_max":6.144,"total_exposure_time":null,"seccolumn":null},"fits":[{"models":[{"model_plot":"https://www.sasbdb.org/media/pdb_file/images/SASDDK9_fit1_model1_img.png","software":"DAMMIF","pdb_link":[],"model_title":null,"type_of_model":"dummy","software_version":"2.7","model_data":"https://www.sasbdb.org/media/pdb_file/SASDDK9_fit1_model1.pdb","model_mw":24.0,"bead_radius":1.2,"log":null,"symmetry":null,"comment":null,"user":323}],"fit_unit":"1/A","fit_plot":"https://www.sasbdb.org/media/fitting_files/scattering_plots/SASDDK9_fit1_fit_img.png","software":"DAMMIF","chi_square_value":1.822,"p_value":0.052545,"fit_residual_plot":"SASDDK9_fit1_fitresiduals_img.png","fit_data":"https://www.sasbdb.org/media/fitting_files/SASDDK9_fit1.fir","fit_log":"https://www.sasbdb.org/media/fitting_files/log_files/BJ_2_10.log","software_version":"2.7","description":null}],"estimated_volume_method":null,"pddf_software":"ATSAS GNOM","pddf_software_version":"2.7","i0_calibration_standard":null,"description":"The sample-to-detector distance (collimation distance) and exposure times used were: 1.4 m (2.8m), 5 min and; 8m (8 m), 20 min. The CRYSON resolution files are included in the full entry zip archive.","experiment_description":"SANS data from solutions of the R1-3 human dystrophin fragment with zwitterionic phospholipid bicelles in 20 mM Tris-d11, 150 mM NaCl, 0.1 mM EDTA-d16, in 100% v/v D2O, pD 7.5 (pH 7.1) were collected on the D22 SANS instrument at the Institut Laue-Langevin (ILL, Grenoble, France) using a 3He multidetector 128 linear sensitive Reuter-Stokes detector detector at two sample-detector distances a neutron wavelength of λ = 0.6 nm (l(s) vs s, where s = 4πsinθ/λ, and 2θ is the scattering angle). One solute concentration of 4.20 mg/ml was measured at 22°C at both sample-detector distances as were appropriate solvent blanks prior to data reduction and merging.","tags":[],"intensity_unit":"1/cm","experimental_mw":45.0,"experimental_mw_error":null,"guinier_i0_mw":null,"guinier_i0_mw_error":null,"porod_mw":null,"porod_mw_error":null,"pddf_i0":0.1709,"pddf_i0_error":null,"guinier_i0":0.17,"guinier_i0_error":null,"pddf_rg":4.43,"pddf_rg_error":null,"guinier_rg":4.1,"guinier_rg_error":0.1,"pddf_dmax":17.8,"pddf_dmax_error":null,"porod_volume":50.0,"porod_volume_error":null,"estimated_volume":null,"estimated_volume_error":null,"guinier_point_first":1,"guinier_point_last":27,"pddf_point_first":null,"pddf_point_last":null,"i0_calibration_standard_data":null,"intensities_log_log_plot":"SASDDK9_datloglog_img.png","symmetry":null,"last_modified":"2022-08-15T14:51:04.900446+02:00","bragg_peak":[]}