{"code":"SASDFA4","status":"Published","type_of_curve":"Single concentration","angular_unit":"1/nm","project":{"title":"The quaternary structure of insulin glargine and glulisine under formulation conditions.","publication":{"title":"The quaternary structure of insulin glargine and glulisine under formulation conditions.","author_list":"Nagel N, Graewert MA, Gao M, Heyse W, Jeffries CM, Svergun D, Berchtold H","journal":"Biophys Chem","doi":"10.1016/j.bpc.2019.106226","pmid":"31376619","published_date":"2019 Oct"},"status":"released","submitted_date":"2019-03-20","released_date":"2019-07-26"},"pddf_data":"https://www.sasbdb.org/media/p_of_R_files/SASDFA4.out","intensities_data":"https://www.sasbdb.org/media/intensities_files/SASDFA4.dat","intensities_log_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDFA4_dat_img.png","intensities_kratky_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDFA4_kratky_img.png","pddf_plot":"https://www.sasbdb.org/media/p_of_R_files/pofr_images/SASDFA4_pofr_img.png","intensities_guinier_plot":"https://www.sasbdb.org/media/intensities_files/scattering_plots/SASDFA4_guinier_img.png","sascif_data":"https://www.sasbdb.org/media/sascif/sascif_files/SASDFA4.sascif","experiment":{"instrument":{"detector":{"type":null,"name":"Pilatus 6M","resolution":null},"name":"PETRA III","city":"DESY; 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Mixture analysis of the scattering profiles was  performed with the program Oligomer. Data can be fit with a stable equilibrium of ~ 60 % hexamers (based on 1ev3.pdb) and ~ 40 % dimers. For higher concentration a strong influence of \r\ninterparticle interference is observed, so that data at low s (>0.05 nm-1) is omitted for the fit. The presence of 3% dodecamers (based on 3W80.pdb) \r\nslightly improves the fit.","experiment_description":null,"tags":[],"intensity_unit":"arbitrary","experimental_mw":35.0,"experimental_mw_error":null,"guinier_i0_mw":35.0,"guinier_i0_mw_error":194.0,"porod_mw":null,"porod_mw_error":null,"pddf_i0":692.9,"pddf_i0_error":null,"guinier_i0":658.24,"guinier_i0_error":3.72,"pddf_rg":1.9,"pddf_rg_error":null,"guinier_rg":1.8,"guinier_rg_error":0.1,"pddf_dmax":6.2,"pddf_dmax_error":null,"porod_volume":null,"porod_volume_error":null,"estimated_volume":null,"estimated_volume_error":null,"guinier_point_first":1,"guinier_point_last":null,"pddf_point_first":null,"pddf_point_last":null,"i0_calibration_standard_data":null,"intensities_log_log_plot":"SASDFA4_datloglog_img.png","symmetry":null,"last_modified":"2023-06-21T07:55:24.740692+02:00","bragg_peak":[]}