data from solutions of
Microtubule affinity regulating kinase (isoform MARK1)
0.1 M Bis-Tris, 0.2 M ammonium citrate, 1mM DTT, pH 6.5
EMBL X33 beam line
at the DORIS III, DESY storage ring
using a MAR 345 Image Plate detector
at a sample-detector distance of 2.7 m and
at a wavelength of λ = 0.15 nm
(I(s) vs s, where s = 4πsinθ/λ, and 2θ is the scattering angle).
Solute concentrations ranging between 0.5 and 6 mg/ml were measured
120 second frames were collected.
The data were normalized to the intensity of the transmitted beam and radially averaged; the scattering of the solvent-blank was subtracted.
The low angle data collected at lower concentration were merged with the highest concentration high angle data to yield the final composite scattering curve.
Cell temperature = UNKNOWN. Storage temperature = UNKNOWN