Extended q‐range X‐ray Scattering Reveals High‐Resolution Structural Details of Biomacromolecules in Aqueous Solutions

Chen J, Borkiewicz O, Grishaev A, Zhang F, Bera M, Ruett U, Levin I
Chemistry – A European Journal (2023 Jan 16)

doi: 10.1002/chem.202203551

Submitted to SASBDB: 2023 Jan 9 Published in SASBDB: 2023 Jan 17

SASDR82 – Alpha cyclodextrin - 50 mg/ml aqueous solution measured to 235 inverse nm Sample: Alpha cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.6 nm

SASDR92 – Alpha cyclodextrin - 25 mg/ml aqueous solution measured to 235 inverse nm Sample: Alpha cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.6 nm

SASDRA2 – Alpha cyclodextrin - 12.5 mg/ml aqueous solution measured to 235 inverse nm Sample: Alpha cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.6 nm

SASDRB2 – Beta cyclodextrin - 18 mg/ml aqueous solution measured to 238 inverse nm Sample: Beta Cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.7 nm

SASDRC2 – Beta cyclodextrin - 12.5 mg/ml aqueous solution measured to 238 inverse nm Sample: Beta Cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.7 nm

SASDRD2 – Gamma cyclodextrin - 50 mg/ml aqueous solution measured to 238 inverse nm Sample: Gamma Cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.7 nm

SASDRE2 – Gamma cyclodextrin - 25 mg/ml aqueous solution measured to 238 inverse nm Sample: Gamma Cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.7 nm

SASDRF2 – Gamma cyclodextrin - 12.5 mg/ml aqueous solution measured to 238 inverse nm Sample: Gamma Cyclodextrin monomer, 1 kDa Buffer: water, pH: 7 Experiment: SAXS data collected at 11-ID-B, Advanced Photon Source (APS), Argonne National Laboratory on 2021 Nov 2 RgGuinier 0.7 nm